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Calcium Saccharin Manufacturer Exporter USP FCC Food Grade Manufacturer Exporter
Crystal Clear Products is a manufacturer exporter company manufacturing several chemicals including Calcium Saccharin and IP BP Ph Eur USP NF JP ACS AR Analytical Reagent FCC Food Grade, Pharmaceutical Chemicals at best prices. The group has offices and factories in India USA and UAE and toll manufacturers in China and sells to almost every country in the world.
The manufacturing facilities of our partner manufacturers have one or more of FDA-cGMP-GLP certification, ISO-9001 certification, Halal and/or Kosher certification, REACH pre-registration ISO-22000 HACCP. We also allow third party inspection of products offered. We can offer small quantities from laboratory and trial packs to large shipments of container loads of material.
Hazard Statements:
H315: Causes skin irritation.
H319: Causes serious eye irritation.
H333: May be harmful if inhaled.
H335: May cause respiratory irritation.
Signal Word: Warning
Transport Information
DOT USA, TDG Canada & ADR/RID Europe: Not dangerous goods.
IMO/IMDG: Not dangerous goods.
IATA/ICAO: Not dangerous goods.
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Calcium Saccharin SDS of Manufacturers
Calcium Saccharin IP BP Ph Eur USP NF FCC Food AR ACS Reagent Grade Manufacturers
CAS Number 6381-91-5 for Hydrate and 6485-34-3 for Anhydrous Calcium Saccharin, Molecular Weight: 467.48, Chemical Formula: C14H8CaN2O6S2-3.5H2O
Saccharin Calcium USP Grade Specifications:
C14H8CaN2O6S2-3½ H2O - 467.48
C14H8CaN2O6S2 - 404.44
1,2-Benzisothiazol-3(2H)-one, 1,1-dioxide, calcium salt, hydrate (2:7);
1,2-Benzisothiazolin-3-one 1,1-dioxide calcium salt hydrate (2:7) CAS 6381-91-5
Anhydrous CAS 6485-34-3
DEFINITION
Saccharin Calcium contains NLT 99.0% and NMT 101.0% of C14H8CaN2O6S2 , calculated on the anhydrous basis.
IDENTIFICATION
A. Infrared Absorption
Sample: Dry at 105C to constant weight.
B. Procedure
Sample solution: 100 mg/mL
Analysis: To the Sample solution add 2 drops of methyl red, and neutralize with 6 N ammonium hydroxide. Add 3 N hydrochloric acid, dropwise, until the solution is acid to the indicator. Add ammonium oxalat.
Acceptance criteria: A white precipitate is formed when the ammonium oxalate is added. This precipitate is insoluble in 6 N acetic acid but dissolves in hydrochloric acid.
C. Calcium salts moistened with hydrochloric acid impart a transient yellowish-red color to a nonluminous flame.
Impurity:
o-Toluenesulfonamide: 10 ppm maximum.
p-Toluenesulfonamide: 10 ppm maximum.
Procedure 2: Limit of Benzoate and Salicylate:
Sample solution: 50 mg/mL
Analysis: To 10 mL of the Sample solution add 5 drops of 6 N acetic acid and 3 drops of ferric chloride.
Acceptance criteria: No precipitate or violet color appears.
Water Determination: NMT 15.0%
Readily Carbonizable Substances:
Sample solution: 40 mg/mL in sulfuric acid (94.5%–95.5% (w/w) of H2SO4), 48C to 50C for 10 min
Acceptance criteria: The Sample solution has no more color than Matching Fluid A, when viewed against a white background.
Clarity of Solution: To pass the test.
Color of Solution: To pass the test.
Packaging and Storage: Preserve in well-closed containers. Store at room temperature.
Calcium Saccharin FCC Food Grade Specifications
1,2-Benzisothiazolin-3-one 1,1-Dioxide Calcium Salt
C14H8CaN2O6S2-31-2H2O Formula weight 467.48
INS: 954 CAS anhydrous 6485-34-3
DESCRIPTION
Calcium Saccharin occurs as white crystals or as a white, crystalline powder. One gram is soluble in 1.5 mL of water.
Function: Nonnutritive sweetener.
REQUIREMENTS
Identification:
A. Dissolve about 100 mg of sample in 5 mL of a 1:20 solution of sodium hydroxide, evaporate to dryness, and gently fuse the residue over a small flame until ammonia no longer evolves. After the residue has cooled, dissolve it in 20 mL of water, neutralize the solution with 2.7 N hydrochloric acid, and filter. Add 1 drop of ferric chloride to the filtrate. A violet color appears.
B. Mix 20 mg of sample with 40 mg of resorcinol, cautiously add 10 drops of sulfuric acid, and heat the mixture in a liquid bath at 200C for 3 min. After cooling, add 10 mL of water and an excess of 1 N sodium hydroxide. A fluorescent green liquid results.
C. A1:10 aqueous solution gives positive tests for Calcium.
D. Add 1 mL of hydrochloric acid to 10 mL of a 1:10 aqueous solution. A crystalline precipitate of saccharin forms. Wash the precipitate well with cold water, and dry at 105C for 2 h. The saccharin thus obtained melts between 226C and 230C.
Assay: Not less than 98.0% and not more than 101.0% of C14H8CaN2O6S2, calculated on the anhydrous basis.
Benzoate and Salicylate: Passes test.
Lead: Not more than 2 mg/kg.
Readily Carbonizable Substances: Passes test.
Selenium: Not more than 0.003%.
Toluenesulfonamides: Not more than 0.0025%.
Water: Not more than 15.0%.
Contact for Monograph, Uses, Matnfacturing Process, etc of Calcium Saccharin and JP IP BP Ph Eur USP NF FCC Food AR ACS Reagent Grade Manufacturer Supplier Exporter
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MUMBAI 400009, INDIA. TEL: (OFFICE) 91-9322665100
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Last updated
11/19/2022
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